毕业答辩PPT模板学术本科生研究生大学生开题报告动态论文答辩(47)

若黑般聚()双单体法两亲性超支化β-环糊精及其性能研究合成反应2d+透析&干燥10d反应2h沉降&干燥2d反应1d+沉降&干燥2d接枝核壳HBPBx-NH2单体Bx-OTs单体HBPPNIPAm-COOH反应4d+透析&干燥10d反应1d沉降&干燥2dHClDMAP吡啶DMF,冰浴24:00Bx-OTsBx-NH2HBP接枝核壳HBPLCSTLCST102030405060708090100-2000200400600800100012001400Diam(nm)T(℃)HBP接枝核壳HBPLCST=52℃CMC28030032034036001000200030004000500060007000ExcitationIntensity(a.u.)Wavelength(nm)40507010011×10-15×10-15×10-21×10-25×10-31×10-35×10-41×10-45×10-51×10-55×10-61×10-6339nm335nmI335/I339logC(mg/ml)-3-2-101110.70.80.91.01.1=0.71mg/mlCMCCMC0.5mg/ml0.4mg/ml0.3mg/ml0.2mg/ml0.1mg/ml5mg/ml4mg/ml3mg/ml2mg/ml1mg/ml4404504604708400860088009000920094009600Wavelength(nm)emissionintensity(a.u.)LL(X×10-5mol/L)pH=7.45mg/ml4mg/ml3mg/ml2mg/ml0mg/ml0.00.51234586008800900092009400Wavelength=457.8nmemissionintensity(a.u.)Concentration(mg/ml)红外核磁DSCTGA测定LCST客体包载荧光