梅特勒电位滴定仪操作介绍

操作介绍全自动电位滴定仪METTLERTOLEDOANAProductApplicationSupportNovember6,20192全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining2滴定分析的要求完全的化学反应快速的反应按固定比例进行反应可测定终点METTLERTOLEDOANAProductApplicationSupportNovember6,20193全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining3滴定的定义滴定是一种化学定量分析用一已知浓度的滴定剂和被测溶液发生完全的化学反应，从而定量测定被测溶液METTLERTOLEDOANAProductApplicationSupportNovember6,20194全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining4电极的信号响应代替人眼对指示剂颜色变化的判断终点判断的方法指示剂的颜色变化手工滴定自动电位滴定METTLERTOLEDOANAProductApplicationSupportNovember6,20195全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining5滴定速度更快速,准确提高结果的重现性减低人为错误自动化进行复杂的滴定程序自动电位滴定的优点METTLERTOLEDOANAProductApplicationSupportNovember6,20196全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining6梅特勒-托利多自动电位滴定仪的基本结构搅拌器测量电极滴定杯键盘滴定管中央控制器METTLERTOLEDOANAProductApplicationSupportNovember6,20197全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining7图象功能键(例：滴定管)•清洗滴定管•清洗滴定管段•馈液•连续馈液菜单操作键(例：基本设置)•滴定剂•传感器•温度传感器•滴定台•周边设备•溶剂•输入控制•输出控制人机工程化特大液晶显示操作面板一目了然！DL5X系列滴定仪方法概念METTLERTOLEDOANAProductApplicationSupportNovember6,20199全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining9仪器如何进行自动滴定？-有效的滴定方法SampleEQPTitrationStirTitleCalculationReportCalculationCalculationMETTLERTOLEDOANAProductApplicationSupportNovember6,201910全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining10如何建立有效的滴定方法SampleEQPTitrationStirTitleCalculationReportCalculationCalculationTitrant/SensorTitrantadditionMeasuremodeRecognitionTerminationEvaluationPredispensingMETTLERTOLEDOANAProductApplicationSupportNovember6,201911全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining11标题:酸含量的测定方法移取5ml样品至烧杯中，加入40蒸馏水.滴加3滴酚酞指示剂.用0.1NNaOH滴定至溶液呈微红色.读取所消耗的0.1MNaOH的体积数.做2次以上的平行样品.计算酸含量可通过以下公式得到:R=64xVxc/Vol计算做3个样品的统计结果报告结果METTLERTOLEDOANAProductApplicationSupportNovember6,201912全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining12•自动滴定仪方法–清晰的文本格式METTLERTOLEDOANAProductApplicationSupportNovember6,201913全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining13滴定方法需由多个步骤组成METTLERTOLEDOANAProductApplicationSupportNovember6,201914全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining14直到现在，滴定方法的建立仍然是滴定工作中最困难的一步METTLERTOLEDOANAProductApplicationSupportNovember6,201915全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining15使用DL5X系列滴定仪使以上的问题都迎刃而解！•因为DL5X系列电位滴定仪具有:–21种标准方法–梅特勒－托利多应用方法METTLERTOLEDOANAProductApplicationSupportNovember6,201916全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining16DL5X系列电位滴定仪具备21种滴定方法结构(标准方法)可覆盖90%以上的滴定工作稍作修改便成为您需要的用户方法(UserMethod)SampleEQPTitrationStirTitleCalculationReportCalculationCalculationMETTLERTOLEDOANAProductApplicationSupportNovember6,201917全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining17梅特勒-托利多应用方法•各种常规应用方法•例：电极校正，pH/ISE测定酸碱滴定，银量法滴定，TAN/TBNNaOH标定，HCl标定•可直接调用•也可稍作修改后，用其它的方法名称储存METTLERTOLEDOANAProductApplicationSupportNovember6,201918全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining18标准方法(21种结构)梅特勒-托利多应用方法用户方法METTLERTOLEDOANAProductApplicationSupportNovember6,201919全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining191Equivalencepointtitration(EQP)2EQPtitration(Ipol/Upol)3Endpointtitration(EP)4EPtitration(Ipol/Upol)5TiterbyEQPtitration6TiterbyEPtitration7TiterbyEPtitration(Ipol/Upol)8TiterbyEQPtitration(Ipol/Upol)9BlankbyEQPtitration10BlankbyEPtitration11BlankbyEQPtitration(Ipol/Upol)12BlankbyEPtitration(Ipol/Upol)21种标准方法METTLERTOLEDOANAProductApplicationSupportNovember6,201920全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining2013StattitrationpH-ormV-stating14EQPtitrationwithdispense15EPtitrationwithdispense162Steptitration(EQP)172Steptitration(EP)18CombinedEP/EQPtitration19Sensorcalibration20Sensormeasurement21Learntitration21种标准方法METTLERTOLEDOANAProductApplicationSupportNovember6,201921全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining21•根据您的测试需要作出您的选择–选择最适合你的滴定方法SampleStirTitleReportCalculationCalculationDispenseEQPTitrationSampleEQPTitrationStirTitleCalculationReportCalculationCalculationSampleStirTitleCalculationReportCalculationCalculationEPTitrationSampleStirTitleReportCalculationCalculationDispenseEQPTitrationSampleStirTitleReportCalculationMeasureCalibrationSampleStirTitleReportCalculationpH-statCalculationSampleStirTitleReportCalculationMeasureCalculationMETTLERTOLEDOANAProductApplicationSupportNovember6,201922全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining22若需要建立特殊或更复杂的应用方法METTLERTOLEDOANAProductApplicationSupportNovember6,201923全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining23DL58/DL70ES/DL77的灵活方法结构概念可满足您的需要！METTLERTOLEDOANAProductApplicationSupportNovember6,201924全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining24SampleEQPTitrationStirTitleCalculationReportCalculationCalculation•标准方法的结构滴定步骤METTLERTOLEDOANAProductApplicationSupportNovember6,201925全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003CustomerTraining25•理解每个菜单的含义SampleStirTitleCalculationEQPTitrationMETTLERTOLEDOANAProductApplicationSupportNovember6,201926全自动电位滴定仪TitratorKFTitratorDE/REFPSTARe2003Cu