X射线萤光光谱仪(XRF)检验规范

ThisdocumentandinformationhereinisthepropertyofUSIandallunauthorizeduseandreproductionisprohibited.CopyrightbyUniversalScientificIndustrialCo.,Ltd.機密等級:機密USIControlledDocumentConfidentialLevel:ConfidentialDocumentTitle(文件名稱):X-Rayfluorescencetestspecification(X射線螢光光譜儀(XRF)檢驗規範)DocumentNumber(文件編號):AT-0801-M427Revision(文件版本):A6ReviseDate:6/26/2009Preparedby(撰寫者):EdwinHuang黃基泉CreatebywhichUnit(制定單位):CQM/GRM/GDAG-0801-M006-F2Rev.:A1ThisdocumentandinformationhereinisthepropertyofUSIandallunauthorizeduseandreproductionisprohibited.CopyrightbyUniversalScientificIndustrialCo.,Ltd.AmendmentRecordsItem:Date:Revision:Page:ChangeDescription:Changedby:103/31/2005A26,71.DeletetheCrfromtheitemofXRFtest.2.Addremark.EricChang204/10/2006A371.Addremark3EricChang304/10/2006A36包裝材料的測試值修改為:鉛+汞+鎘+铬需小於100ppm,其中需鎘小於5ppmEricChang405/05/2006A1AllCodingchangefromTT-0801-Q095toTT-0801-M401EricChang505/05/2006A16,71.修改附件一XRF測試零件及產品類別之有害物質限值表規格之Pb,Cr,Hg:700ppm，增加Cd:60ppm之管制2.刪除Remark對Cr暫不設定管制上限之規定EricChang607/05/2006A1All1.DocumentcodingchangefromTT-0801-M401-A1toAT-0801-M427-A1.2.Addthepurposeandscope.KenKe柯炤榕711/30/2006A22,4,111.OmitthatthisprogramispracticableinTaiwanandChinasites.2.ModifyMethod3:testpointofPCB.3.RemovePackageitemonattachment1:theCdmustunder5ppm.EdwinHuang804/29/2008A310,121.AddhalogenfreeandSpottestitems.2.DeleteBrcontrollingitem.EdwinHuang908/20/2008A41,10,12~141.Addattentionitemsforthetoolmanagementprocessofmechanicalpreparation.2.Addtheflowchartandformforthemanagementprocesstoattachment.EdwinHuang1009/04/2008A510~12UpdatedAttachment1:EHSthresholdvalueofcomponenttypeforXRFtestEdwinHuang1106/26/2009A61011121.Addtestmethodifcustomerrequest2.Delete”IQCwon’tcontrolthethresholdvalueofCl..3.Add“Ifthematerialcomposedofmetal,glassandceramic.ThecomponentEdwinHuangThisdocumentandinformationhereinisthepropertyofUSIandallunauthorizeduseandreproductionisprohibited.CopyrightbyUniversalScientificIndustrialCo.,Ltd.14won’tbecarriedouthalogenfree..4.UpdatedAT-0801-M427-F1toA2version.AG-0801-M006-F3Rev.:A111SourceOrganization：USI/TaiwanX-RayfluorescencetestspecificationX射線螢光光譜儀(XRF)檢驗規範DOCNO.:AT-0801-M427-A6OriginalEffectiveDate：03/31/2005PAGE1of14ThisdocumentandinformationhereinisthepropertyofUSIandallunauthorizeduseandreproductionisprohibited.CopyrightbyUniversalScientificIndustrialCo.,Ltd.目錄Content一、目的Purpose二、適用範圍Scope三、樣品檢測條件及方法Testcondition&methodforsample四、零件及產品測試原則TestingRule五、測試方法TestMethod六、注意事項Attentionitem七、附件Attachment1.XRF測試零件及產品類別之有害物質限值表限值表EHSthresholdvalueofcomponenttypeforXRFtest2.拆解治工具管理流程Themanagementprocessfordisassemblytoolsofthecomponent.3.XRF治工具季驗證紀錄表(AT-0801-M427-F1)TherecordofdisassemblytoolsinquarterinspectionbyXRF(AT-0801-M427-F1).22SourceOrganization：USI/TaiwanX-RayfluorescencetestspecificationX射線螢光光譜儀(XRF)檢驗規範DOCNO.:AT-0801-M427-A6OriginalEffectiveDate：03/31/2005PAGE2of14ThisdocumentandinformationhereinisthepropertyofUSIandallunauthorizeduseandreproductionisprohibited.CopyrightbyUniversalScientificIndustrialCo.,Ltd.目的：Purpose本規範在建立進料之XRF檢驗標準，以確保品質合乎既定之標準。ThepurposeofthisprogramistoestablishthespecificationoftheXRFinspectionforincomingmaterialstoassurethequalityofmaterialsandcomplywithspecifiedcriteria.一、適用範圍：Scope適用於各大類零件之檢驗。Applytoalltypesofmaterials.二、樣品檢測條件及方法：Testcondition&method1.分析方法分為檢量線法及FP法，說明如下：TestmethodscanbeseparatedtothemethodofcalibrationcurveandFPmethod.1.1.檢量線法：對應於XRF之分析條件為”Cd,Pb,Hg,Br,Cr.bcc”，適用之材質為塑料、紙張、木材及Mg,Al,Si較輕元素)為主材質之樣品。Methodofcalibrationcurve:Themethodisusedforplastic,paper,woodandsomematerialsmainlycomposingofMg,Al,andSi.Theanalysisconditionis”Cd,Pb,Hg,Br,Cr.bcc”.1.2.FP法：對應於XRF之分析條件為”metal2.bfb”，適用之材質為金屬(較重元素)為主材質之樣品。FPmethod:Themethodisusedforsomematerialsmainlycomposingofheavymetal.Theanalysisconditionis”metal2.bfb”.四、零件及產品測試原則：TestingRule1.金屬及塑料共存者:平鋪於測試台並裁切至適當尺寸測試之。Thesamplecomposedofmetallicandplasticmaterials:Cutthesampletobesuitablesizeinthetestplatform.2.形狀凹凸不平者：測試點過高(超過0.5cm)時須拆解樣品，再取平整面測試(約1cm×1cm)。Thesurfacenotbumpy:Separatethesamplewhilethetestpointishigherthantestplatform(0.5cm).3.條狀金屬線者:依其縱方向排列於測試台測試之。Themetallicsampleshapedintobartype:Arrangeitverticallyintestplatform.4.鮮豔紅、黃、橙色者:應優先量測(如油墨、塑膠類、PVC等)。Thesamplepaintedbybrightlyred,yellowandorangecolor:Measurethepointfirst(suchasink,plasticandPVC).33SourceOrganization：USI/TaiwanX-RayfluorescencetestspecificationX射線螢光光譜儀(XRF)檢驗規範DOCNO.:AT-0801-M427-A6OriginalEffectiveDate：03/31/2005PAGE3of14ThisdocumentandinformationhereinisthepropertyofUSIandallunauthorizeduseandreproductionisprohibited.CopyrightbyUniversalScientificIndustrialCo.,Ltd.五、測試方法：TestMethod:Method1：1.DIP類測試方法：以檢量線法測試。DIP:testbythemethodofcalibrationcurve.1.1.本體大於1cm時：以本體為主並包括部分接腳進行測試(請參閱圖1)。Samplesize1cm:Focusonbodyandincludespartialterminal(Refertofigure1).1.2.本體小於1cm時：包含本體及接腳測試(請參閱圖2)。Samplesize1cm:Includingthewholebodyandterminal(Refertofigure2).Method2：以檢量線法測試。Testbythemethodofcalibrationcurve.2.SMD類：分為長(L)，寬(W)，高(H)2mm類及其他尺寸類。SMD:Dividesampleintotwotypes,oneisLength(L),width(W),orheight(H)2mm,DIP類DIPtype本體包含接腳之影像視窗圖Thetestimageincludingb