一步法合成葡萄糖酸钙

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(),,,82.1%,pH.;;;TQ460.31;TQ426.820:19960902:,19572,.,;,1,.,[1].,[24].,,,.,[2].,,.,[3],,,[4].,,,.11.1:,.:.:.1.2,,,,.:C6H12O6O2C6H12O7Ca(OH)2Ca(C6H11O7)2õH2O1.31..1000mL,110g,0.40kgöm3,2.2g,,20119983JOURNALOFWUHANINSTITUTEOFCHEMICALTECHNOLOGYVol.20No.1Mar.1998©1994-2006ChinaAcademicJournalElectronicPublishingHouse.Allrightsreserved.öh.8h,,95%,.,,6#,,.,1.10,,4#,,,.,803%,.(É),,,.90.1g.22.1,.10,82.1%,1.1ögög(%)9200111080920021105092003120869200411065.99200511081.19200612085.79200711082.29200811081.69200911082.39201011082.1:67.0:72.084.961.382.872.185.983.487.887.287.987.71120780.9139.082.12.22.2.10.40kgöm3pH104570Löh1600römin,,2.2,2%.,.2.2.2,,,,3.3,0320©1994-2006ChinaAcademicJournalElectronicPublishingHouse.Allrightsreserved.[5].1600römin,95%.3,,,,,,,.,,,,.,,,,.131:©1994-2006ChinaAcademicJournalElectronicPublishingHouse.Allrightsreserved.:,1986.2..,1988,(4):32333,..,1989,(3):14194..,1992,(4):16195JutaroOkada..,1969,(7):13261337TheSynthesisofCalciumGluconatebytheOneStepProcessChenJianchu(DepartmentofScienceandTechnical,WuhanInstituteofChemicalTechnology,Wuhan430073,China)AbstractAnewmethodofthepreparingcalciumgluconateispresentedbythecatalyticoxi2dationoftheglucose.Theyieldofcalciumgluconatewas82.1%.Theeffectsofcatalysis,concentrationofglucosesolution,temperature,pHetc.onthetransformationofglucosehavebeenstudied.Keywordsglucose;catalyticoxidation;calciumgluconate;technology2320©1994-2006ChinaAcademicJournalElectronicPublishingHouse.Allrightsreserved.

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