高效液相色谱法测定含量时关于确立色谱条件与溶液浓度的讨论

200894288DrugStandardsofChina2008,vol19No14:,,::021-38839900-26303(,201203),,:(HPLC);;;;:92112:A:1009-3656(2008)-3-288-2DiscussionaboutChromatographicConditionsandSolutionConcentrationinContentDetermina2tionbyHPLCXieMu2feng(ShanghaiInstituteforDrugControl,Shanghai201203),,,1/10,,,1,(),,([1,2]);,(),HPLC,,,:,;,(,1/100),,;,,[3],,(22=82151)40min,,,:2(11),10min;1/1002,,,,(DrugStandardsofChina2008,vol19No14200894289),[3],210nm,,240nm()220nm()3,1/10,(6RSD210%)(100%,10%200%,01999)();HPLC1106107(),,(015mgL-1),,1/201/50,:(1),,;,;,,,,,!(2),,,,:(1/5),50mL,,;:1,10mL,,,,255%,,,,10mL,10mL,;:1,100mL,215;10mL,(3),,,,(,,),;,,,,,,;,(),,,:510,,,100,,,,,,(4),,,,,,(),,,,,,(1/201/50)[1]11,20071(38)1[2]11,2003111[3]RP2HPLC11,2002133(7):34123431