气质联用法测定纺织助剂中有机氯载体的含量-卫敏

??®????®????®DeterminationoftheContentofOrgano-ChlorideCarriersinTextileAuxiliariesviaGC-MSMethodWEIMin(FujianProvincialFiberInspectionBureau,Fouzhou350026,Fujian,China)Abstract:Amethodforthedeterminationoforgano-chloridecarriersintextileauxiliariesbyusingGC-MStogetherwithsolidphaseextractionwasestablished.Themethodhasbeensuccessfullyusedtodetermine23organo-chloridecarriersintextileauxiliarieswitharecoveryof73%~98%,arelativestandarddeviation(RSD)of2.8%8.5%andadetectionlimitof0.70?g/kg~1.77?g/kg,indicatingthatourmethodhasalowerdetectionlimit,goodaccuracyandhighprecision.Keywords:textileauxiliary;organo-chloridecarrier;GC-MS???DeterminationoftheContentofOrgano-ChlorideCarriersinTextileAuxiliariesviaGC-MSMethodWEIMin(FujianProvincialFiberInspectionBureau,Fouzhou350026,Fujian,China)Abstract:Amethodforthedeterminationoforgano-chloridecarriersintextileauxiliariesbyusingGC-MStogetherwithsolidphaseextractionwasestablished.Themethodhasbeensuccessfullyusedtodetermine23organo-chloridecarriersintextileauxiliarieswitharecoveryof73%~98%,arelativestandarddeviation(RSD)of2.8%8.5%andadetectionlimitof0.70?g/kg~1.77?g/kg,indicatingthatourmethodhasalowerdetectionlimit,goodaccuracyandhighprecision.Keywords:textileauxiliary;organo-chloridecarrier;GC-MS???