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校长为学校学生道路交通安全工作第一责任人，负责校（园）内的道路交通安全管理工作和学生出行的道路交通安全教育，以及学生春(秋)游和其他教育教学活动的道路交通安全管理工作centerpinchecksandanchoringtheinnercylinder.AccordingtoWhilecouplingalignmentshouldkeepoiloutofcavityandlocatetherotoraxisneckraisedarewithintheprescribedlimits,thereshouldbenogaps,Horn,HornandHorn0.05mmfeelergaugesfitinto.Centercoupling,condenserwaterfillingandwater-filledaccordingtofactoryrequirement.ForcouplingthreesupportedrotorCenter,themouthunderthecouplingbetweenthevalueshouldbeasstipulatedinthemanufacturer,usually0.15~0.25mm.Inthecaseofcouplingconnection,ifpossible,liftingonlyonebearingendofthesupportbearingoftherotor,removethebearing,fittedwithspecialtilesandspecialliftingtools,discrotors,checkthejournalfluttertile,shouldgenerallybelessthan0.10MM.Whenthecouplingsandrotorcomeswhenthereisaconflict,thecouplingCentreshallprevail.6.4.5.2.2shaftlookingfor:...6.4.5.3.Provisionalboltconfirmedthepositioningoftherotorsize,aswellasthecouplingbetweentheadjustmentshimthicknessaccuracy,drawingstomeetthetechnicalrequirements.Plane,cylindricalandcleanthecouplingboltholesshouldbecleanandwithoutburrs,scrapironandgrease-free,relativepositionofthecouplingaccordingtothedrawingrequirementsare.Couplingtopscrews,rounddistanceapart,indicatorstomonitormovementoftheaircraft,itsvalueisallowedtopassthevalueaxismoving,mountedadjustmentpads,notepadsinstallationdirectionguidepincouplingwithprocessendclosed.Thebackwheelsslowlytightened,when2mmorso,withstandardwhitebarswheretwobackwheelboltholemeasurementaboveandbelow,confirmtwobackwheelboltholeconcentricity.Then,thesymmetricalhorizontalmounttwotemporaryboltstightened,attentiontomonitordialindicator,theninstallthesymmetricaltemporarybolts,thistimesitesslowlymovingrotor,inthemeasuredcircumferenceof8equalpartsbackwheelrimrock,eachmeasuringrelativechangesinvalueshouldbelessthan0.02mm.6.4.5.4couplingreamedandpairedboltreamingdiereamer,adjustablereamers,boringmill,inseveralways.6.4.5.4.1Generalrequirementsbeforereamingorboring,九年级中考化学复习专题气体的制取、收集、净化和干燥一、常见气体的实验室制法：气体氧气（O2）氢气（H2）二氧化碳（CO2）药品加热高锰酸钾（KMnO4）或双氧水（加二氧化锰作催化剂）[固（+固）]Δ锌粒（Zn）和稀硫酸（H2SO4）[固+液]石灰石（大理石）（CaCO3）和稀盐酸（HCl）[固+液]反应原理2H2O22H2O+O2↑2KMnO4==K2MnO4+MnO2+O2↑Zn+H2SO4=ZnSO4+H2↑CaCO3+2HCl=CaCl2+H2O+CO2↑发生装置检验用带火星的木条,伸入集气瓶,若木条复燃,是氧气；否则不是氧气点燃，罩干冷小烧杯，产生淡蓝火焰，杯内壁有水珠，则该气体是氢气通入澄清的石灰水，看是否变浑浊，若浑浊则是CO2。收集方法①排水法(不易溶于水)②瓶口向上排空气法(密度比空气大)①排水法(难溶于水)②瓶口向下排空气法(密度比空气小)①瓶口向上排空气法(密度比空气大)（不能用排水法收集）验满验纯验满：用带火星的木条,平放在集气瓶口,若木条复燃,氧气已满,否则没满验纯：1用拇指堵住集满氢气的试管口；2靠近火焰,移开拇指点火；若“噗”的一声，氢气已纯；若有尖锐的爆鸣声，则氢气不纯验满：用燃着的木条,平放在集气瓶口,若火焰熄灭,则已满；否则没满放置正放倒放正放注意事项①检查装置的气密性②试管口要略向下倾斜(防止凝结在试管口的小水珠倒流入试管底部使试管破裂)③加热时应先使试管均匀受热，再集中在药品部位加热。④排水法收集完氧气后,先撤导管后撤酒精灯(防止水槽中的水倒流,使试管破裂)⑤用高锰酸钾制取氧气时，试口要塞一团棉花。防此高锰酸钾进入导管。①检查装置的气密性②长颈漏斗的管口要插入液面下；③点燃氢气前，一定要检验氢气的纯度（空气中，氢气的体积达到总体积的4%—74.2%点燃会爆炸。）①检查装置的气密性②长颈漏斗的管口要插入液面下；③不能用排水法收集小结：1、气体的发生装置（常用发生装置、选择依据、气密性的检验方法）（1）常用发生装置类型：①、固＋固，加热型（一定要用酒精灯）(图1)校长为学校学生道路交通安全工作第一责任人，负责校（园）内的道路交通安全管理工作和学生出行的道路交通安全教育，以及学生春(秋)游和其他教育教学活动的道路交通安全管理工作centerpinchecksandanchoringtheinnercylinder.AccordingtoWhilecouplingalignmentshouldkeepoiloutofcavityandlocatetherotoraxisneckraisedarewithintheprescribedlimits,thereshouldbenogaps,Horn,HornandHorn0.05mmfeelergaugesfitinto.Centercoupling,condenserwaterfillingandwater-filledaccordingtofactoryrequirement.ForcouplingthreesupportedrotorCenter,themouthunderthecouplingbetweenthevalueshouldbeasstipulatedinthemanufacturer,usually0.15~0.25mm.Inthecaseofcouplingconnection,ifpossible,liftingonlyonebearingendofthesupportbearingoftherotor,removethebearing,fittedwithspecialtilesandspecialliftingtools,discrotors,checkthejournalfluttertile,shouldgenerallybelessthan0.10MM.Whenthecouplingsandrotorcomeswhenthereisaconflict,thecouplingCentreshallprevail.6.4.5.2.2shaftlookingfor:...6.4.5.3.Provisionalboltconfirmedthepositioningoftherotorsize,aswellasthecouplingbetweentheadjustmentshimthicknessaccuracy,drawingstomeetthetechnicalrequirements.Plane,cylindricalandcleanthecouplingboltholesshouldbecleanandwithoutburrs,scrapironandgrease-free,relativepositionofthecouplingaccordingtothedrawingrequirementsare.Couplingtopscrews,rounddistanceapart,indicatorstomonitormovementoftheaircraft,itsvalueisallowedtopassthevalueaxismoving,mountedadjustmentpads,notepadsinstallationdirectionguidepincouplingwithprocessendclosed.Thebackwheelsslowlytightened,when2mmorso,withstandardwhitebarswheretwobackwheelboltholemeasurementaboveandbelow,confirmtwobackwheelboltholeconcentricity.Then,thesymmetricalhorizontalmounttwotemporaryboltstightened,attentiontomonitordialindicator,theninstallthesymmetricaltemporarybolts,thistimesitesslowlymovingrotor,inthemeasuredcircumferenceof8equalpartsbackwheelrimrock,eachmeasuringrelativechangesinvalueshouldbelessthan0.02mm.6.4.5.4couplingreamedandpairedboltreamingdiereamer,adjustablereamers,boringmill,inseveralways.6.4.5.4.1Generalrequirementsbeforereamingorboring,2②、固＋液，不加热型（一定不需要酒精灯）ABCDEF注意：①图Ｂ、C、F使用长劲漏斗，必须将长劲漏斗的下端管口插到液面下，形成“液封”，以防气体逸出。②图E使用分液漏斗，图B使用有孔塑料板和带活塞的导管是为了控制反应的速率。（2）气体发生装置的选择依据：由反应物状态和反应条件决定。①若反应物只有固体，且需要加热，应选择图1所示的装置。例如，用高锰酸钾或用氯酸钾与ＭｎＯ２的混合物加热制氧气可选择此装置。（注意：