搜索
Waters2695-2489HPLC2695-2489EmpowerProjectRunSamplesDevelopMethods,MonitorRunSamplesEmpower21.602.11.33.21.44.1.950%50%5.026952695WETPRIME/systempsiWETPRIME/DeltapsiWETPRIME1080911010198127.5mL/min210500abb1340aba1010b30%H3PO420pH101.21.31.41.11.61.71.81.91.101.51.1(PoweringOn)1.Alliance26952489ON(1)2.5“Idle”:BannerAreaDataAreaMenu/StatusScreenKeysMenuScreenKeyszDevelopMethodzRunSamplezDiagzConfigzLog5“Idle”“”“Remote”“”Empower5Log“”Status/Control(1)Status(1)z(Degasser)z(FlowRate)z(SolventComposition)(2)Status(2)z(Deltapsi)“NextPage”Status(1)Status(2)1.2(PreparingSolventReservoirs)z()(18.2MΩ)z48100%z66z(GradientProportioningValve)2695z(SealWash)5%-10%zNeedleWash50%50%*:zz0.45m1z玻1.3(PrimingthePlungerSealWashPump)1.MenuDiag2.SealWash3.PrimeSealWashStartHalt4.Close1.4(PrimetheNeedleWashPump)zzInjectorSealzzz50%50%100%1.MainDiagPrimeNdlWash2.30StartAgain(Sealwash)()1.5(Degasser)1.“Menu/Status”Status(1).2.“Degasser”Enter3.ON1.6(DryPrime)DryPrime1.(Detector)SampleLoop2.(SolventFilter)3.Prime/Ventvalue(3)4.“Menu/Status”Status(1)“DirectFunction”DrydegassermodeONDryPrimePrimeEnter5.(:OpenA)5~10mLPrime/Vent6.”Enteraduration”3“Continue”3.0mL/minPurge7.DryPrime.1.7(WetPrime)WetPrime1.“Menu/Status”Status(1)“Composition”WetPrime100%.2.“DirectFunction”WetPrimeEnterWetPrimeFlowRate:7.5mL/minTime:3.0min“OK”WetPrime3.WetPrime1.81.“Menu/Status”Status(1)“Composition”NewComposition2.“ChangeComp”changecomposition3.“Flow”*:1.9.(PurgeInjector)zzz1.“Menu/Status”Status(1)50%50%2.“DirectFunction”PurgeInjectorEnter3.SampleLoop(6)Enter4.(CompressionCheck)OK1.10.(LoadingCarousels)A1–24B25–48C49–72D73–96E97-120zzNextz.z“”Symmetry/Sunfire100a)b)0.1ml/min10051ml/minc)d)be)f)595300.1ml/min1ml/ming)h)z10250×4.6mm4.2ml1ml/min42z0.1ml/minzz70/254nm248604545245953060zz200µlDMSOz10HPLC18MΩ100“”21.2.3.4.5.6.7.AB135-402345800820267667A)B)(1-5)1.2.3.4.5.1234(30%,,)5,800-820-26761.2.3.4.121.0ml/min3435-405.6.A).B).C).D).7.PURGE8.9.56A).B).(30%,,)C).D).7891.2.3.pH1.2.SunfireXBridge3.pH28pH2695µmmL/minpsipsiSunfireC183.9*150mm54010%:90%10mM19505050psi2695