*1,1,2,1(1.,570228;2.):,,,,,:;;:TQ021.9:A:1006-4990(2010)11-0001-03Researchprogressinpreparationofnano-materialsbyultrasonicmethodsChengXinfeng1,FuYunzhi1,2,ZhangXiaojiao1(1.SchoolofMaterialsScienceandChemicalEngineering,HainanUniversity,Haikou571737,China;2.StateKeyLaboratoryofColloidsandSurfaces,InstituteofChemistry,ChineseAcademyofSciences)Abstract:Chemicalultrasonictreatmentasaneffectivetechniqueforthepreparationofnano-materialshasattractedmoreandmoreattentionsofscientificresearchers.Majormethodsthatapplyingultrasonictechniqueinthepreparationofnano-materialsweregenerallyintroduced.Researchprogressinthepreparationofnano-materialsbyultrasonicmethodsinrecentyearswaselaborated.Inaddition,asummarywasgivenaboutthemechanismanduniversalityalreadyacquiredoftheultrasonicpreparationofnano-materials,meanwhile,thekeyactionofultrasonicconditionsoncontrollingmorphologyandparticlesizeofnano-materialsbydifferentpreparationmethodswasalsodiscussed.Atlast,developmentofultrasonictechniqueinthepreparationofnano-materialsinfuturewasproposed.Studywillprovideareferencefortheresearchonthepreparationofcontrollablenano-materials.Keywords:chemicalultrasonictreatment;nano-materia;lultrasonicprecipitationmethod,,[1],,,,[2],1,,,,,,,,,,2760!5.05∀108Pa,543.3!/s,400km/h,,,,*:(20543001);(Hjkj2009-13)1第42卷第11期2010年11月无机盐工业INORGANICCHEMICALSINDUSTRY2,,,,,,,,[3],,,,2.1,,,,,[4],LaCoO3,,30nm;LaCoO3,,12nmSEM,LaCoO3,,ABO3(A,B),LaCoO3[5]26nmZnO[6]CuS,,20~40nm,,,[7],,30nm10nm(-FeOOH),[8]15nmSb2O3[9]Sb2O3,20nm,,,200!3hSb2O3,,,2.2,,[10],,[11]-Ni-Al2O3,,Al2O3,,,,[12]-Ni2CeO2,,,,-,Ni2CeO22.3,,,[13],,,[14],,(MMA),,45~60nm,[15],ZnO,[16],,,-(PBA/SiO2,PBMA/Al2O3,PMMA/TiO2,PANI/SiO2,PANI/TiO2,PSt/Fe3O4)TEM,,,,2无机盐工业第42卷第11期,,[17]/,BA/AM/SiO2BA/AM/TiO2BA/AM/Fe3O4,/,,2.4,,,R.A.Salkar[18](CTAPTS),(500nm,50nm)[19]-,(CTAB)/(C4H9OH)/(C6H12)/(Na2WO4HCl)40nmWO3,,2.5-,-,,,,[20]-,,3,:1)2)()3),(),,:[1],,.[J].,2004,36(3):45-47.[2],.[J].,2007,39(7):8-11.[3],.[J]..2001,5:268-269.[4],.LaCoO3[J].,1998,11(4):375-378.[5].[J].,2005,37(5):23-24.[6],,,.-CuS[J].:,2006,21(4):12-15.[7],.-[J].,2005,35(2):31-33.[8],,,.Sb2O3[J].,2005,21(3):441-445.[9],,,.-Co3O4[J].,2004,35():3057-3061.[10],,,.[J].,2009,40(5):850-852,857.[11],,.-Ni-Al2O3[C]#.:,2005:322-325.[12],,,.-Ni-CeO2[J].,2009,29(4):313-316.[13]SuslickKS.Sonochemistry[J].Science,1990,247(4949):1439-1445.[14].P/MMA[D].:,2006.[15].-[J].:,2009,32(5):654-657.[16],,./[J].:,2006,38(3):105-109.[17]./[D].:(下转第13页)32010年11月程新峰等:超声法制备纳米材料的研究进展,,-6,2.3,,,[9]2.4,,,,,[6]50%,,,,,[10],5%,,,,[10],,3,,,[11],,:[1],.ABS[J].,2007,19(3):1-5.[2].[EB/OL].,[2010-09-21]=124.[3].[D].:,2004:15-17,28-29.[4],,.:,101311372[P].2008-11-26.[5],.[J].,2002,30(S1):93-95.[6],,,.[J].,2006(6):17-21.[7].[EB/OL].(2007-04-02)[2010-09-21][8],.PP[J].,2005,17(1):35-38.[9],,,.[J].,2004,33(1):4-8.[10],.[J].,2000(3):32-33.[11],.[J].,2006(1):80-83.:2010-08-03:(1963∃),,,,30::zzyf2004@tom.com(上接第3页),2005.[18]SalkarRA,JeevanandamP,KatabyG,eta.lElongatedcoppernanoparticlescoatedwithazwitterionicsurfactant[J].Phys.Chem.B,2000,104:893-897.[19],,,.-WO3[J].,2007,41(1):75-77,94.[20],,.-[J].,2005,22(2):87-91.:2010-06-09:(1986∃),,,::yzhfu@hainu.edu.cn132010年11月刘志彬等:镁盐晶须的应用与开发