Rezex系列色谱柱分析产物解析

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Rezex™tttBio-RadAminext®,SupelcoSupelcogel™WatersSugar-Pak™RCM-Monosaccharide(L19packing)*RHM-Monosaccharide(L17packing)*RAM-CarbohydrateRSO-OligosaccharideRNO-OligosaccharideRPM-Monosaccharide(L34packing)*RNM-Carbohydrate(L58packing)*ROA-OrganicAcid(L22packing)*RFQ-FastAcidRKP-PotassiumRCU-USPSugarAlcohols(L19packing)**UnitedStatesPharmacopeia(USP)㄀义02468101214min1345678201020min13456782Rezex™ttttAppID16650AppID16648RezexROA-OrganicAcid300x7.8mm00H-0138-K00.005NSulfuricAcid0.6mL/minRI@40°C60°CShimadzu™Prominence™LC-20ASystem1.Dp4+5.2.Dp36.3.7.4.8.RezexROA-OrganicAcid150x7.8mm00F-0138-K00.005NSulfuricAcid0.6mL/minRI@40°C60°CShimadzu™Prominence™LC-20ASystem1.Dp4+5.2.Dp36.3.7.4.8.㄀义min10321200min0321122436min35Dp10Dp9Dp8Dp7Dp6Dp5Dp4Dp3Dp2Dp10Dp11Dp12Dp13Dp14min0109876543211020304011min0654321816min06543211224AppID5507AppID5508AppID5505AppID5506AppID5504AppID5515DpRezexRSO-Oligosaccharide200x10mm00P-0133-N00.3mL/minRl75°CRezexRPM-Monosaccharide300x7.8mm00H-0135-K00.6mL/minRI75°C1.2.3.4.5.6.7.8.9.10.11.RezexRCM-Monosaccharide300x7.8mm00H-0130-K00.6mL/minRI75°C1.2.3.RezexRKP-Potassium300x7.8mm00H-3252-K00.4mL/minRI85°C1.2.3.RezexRCM-Monosaccharide300x7.8mm00H-0130-K00.6mL/minRl85°C1.2.3.4.5.6.RezexROA-OrganicAcid300x7.8mm00H-0138-K00.005NSulfuricAcid0.5mL/minUV@210nm55°C1.2.3.4.5.6.Rezex™㄀义min03211020AppID5514MINAppID15501min0432181624AppID5517min543210.0010.0020.0030.00AppID5518min0765432125AppID551010min32110min32110min32144AppID14987,14988,14989RezexROA-OrganicAcid300x7.8mm00H-0138-K00.6mL/minRI1.2.3.RezexRPM-Monosaccharide100x7.8mm00D-0135-K00.6mL/minELSD80°C1.2.RezexROA-OrganicAcid300x7.8mm00H-0138-K01.0mL/minRI40°C1.2.3.4.RezexRCM-Monosaccharide300x7.8mm00H-0130-K00.5mL/minRI60°C1.2.3.4.5.RezexRNM-Carbohydrate300x7.8mm00H-0136-K00.6mL/minRI75°C1.2.3.4.5.6.7.RezexRCM-Monosaccharide300x7.8mm00H-0130-K00.5mL/minELSD80°C1.2.3.4.FRezex™㄀义402006080100120mAU01020min123456402006080100120mAU01020min12345601020min406080100mAU12345601020min406080100120mAU123456100200300400500mAU0246810121416min0246810121416min200400mAU123123AppID14978AppID14963,14962AppID14976AppID14982Rezex™vs.Bio-RadAminex®BaselineResolutionDifficultQuantitation4006080mAU1030min20123450102030min604080100mAU12345RezexRCMAminexHPX-87CRezexRCMAminexHPX-87CRezexROAAminexHPX-87HRezexRCMAminexHPX-87CRezexRCM-MonosaccharideAminexHPX-87C300x7.8mm00H-0130-K00.6mL/minELSD80°C1.2.3.4.5.RezexROA-OrganicAcidAminexHPX-87H300x7.8mm00H-0138-K00.005NH2SO40.5mL/minUV@210nm40°C1.2.3.4.5.6.RezexRCM-MonosaccharideAminexHPX-87C300x7.8mm00H-0130-K00.6mL/minELSD80°C1.2.3.4.5.6.RezexRCM-MonosaccharideAminexHPX-87C300x7.8mm00H-0130-K00.6mL/minELSD80°C1.2.3.BarBarRezex32Aminex55Rezex™AppID14975AppID14977AppID14981㄀义RCMMonosaccharideRSOOligosaccharideRNOOligosaccharideRNMCarbohydrateRAMCarbohydrate00H-0130-K000P-0133-N000P-0137-N000H-0136-K000H-0131-K0300x7.8mm200x10mm200x10mm300x7.8mm300x7.8mm8%4%4%8%8%8μm12μm12μm8μm8μm35,000N/AN/A30,00035,0003502002003503506003003006006000.6(seepressure)0.30.30.60.6858585858503B-0130-K003R-0133-N003R-0137-N003B-0136-K003B-0131-K05%CaSO4,Ca(NO3)2,CaCl2100%100%100%100%100%0.60.20.20.40.4857575757512121212120.1MCa(NO3)20.1MAgNO30.1MNaNO30.1MNaNO30.1MAgNO30.20.10.20.20.285-8585854-16-4-164.-164-16RPMMonosaccharideRHMMonosaccharideROAOrganicAcidRFQFastAcidRCUSugarAlcohols00H-0135-K000H-0132-K000H-0138-K000D-0223-K000G-0130-D0300x7.8mm300x7.8mm300x7.8mm100x7.8mm250x4.0mm8%8%8%8%8%8μm8μm8μm8μm8μm35,00035,00050,000(AceticAcid)30,00012,0003503503503503506006006006006000.60.60.61.00.485858585850.005NH2SO40.005NH2SO41-81-81-803B-0135-K003B-0132-K003B-0138-K003B-0223-K003A-0130-D05%HNO3,H3PO45%HNO3,H3PO45%HNO3,H3PO45%CaSO4,Ca(NO3)2,CaCl2100%100%100%100%0.60.60.50.60.2858585858512121212120.1MPb(NO3)20.025MH2SO40.025MH2SO40.025MH2SO40.1MCa(NO3)20.20.20.20.20.285858585854-164-164-164-164-160.005NH2SO40.005NH2SO4Rezex™!21& P( P(P( JQB ㄀义300x7.8mm0.6mL/min80°CRI@40°CPhenomenexRezex™Bio-RadAminex®SupelcoSupelcogel™WatersSugar-Pak™RCM-MonosaccharideHPX-87C125-0095SupelcogelCaSugar-Pak1RHM-MonosaccharideHPX-87H125-0140SupelcogelC-610H&HN/ARPM-MonosaccarideHPX-87P125-0098SupelcogelPbN/ARNM-CarbohydrateHPX-87N125-0143N/AN/ARSO-OligosaccharideHPX-42A125-0097SupelcogelAg1&Ag2N/AROA-OrganicAcidHPX-87H125-0140SupelcogelC-610H&HN/ARFQ-FastAcidFastAcid125-0100N/AN/ARKP-PotassiumHPX-87K125-0142SupelcogelKN/ARCU-USPSugarAlcoholsSugarAlcohols125-0094N/AN/ASecurityGuard™KJO-4282RAMAg+RCMCa+2RNMNa+RHMH+RPMPb+211.5414.9311.1011.1120.1511.9512.7111.4510.2115.8213.0113.5612.6511.2416.478.868.608.498.0211.0011.9013.8211.3912.5915.3211.6421.6111.1010.7133.2512.3115.4911.7812.1419.8212.0513.6511.7610.3117.7112.7513.1912.3011.6516.1911.8711.7311.4710.1914.948.708.408.407.8710.5311.0410.3710.719.6212.9212.5913.3512.149.9818.879.118.748.768.0211.289.279.0

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