,():,0.99910.9993,95.4%100.9%,95.1%103.5%5%(n=5):;;;,,,,SM,,,,,,;,,,N,N2,,,,11.11.1.1:0199mgPmL;:99.5%DMA100gPmLN,N2(DMA):,,100DMA,,,1.2VARIANCP3800(FID):DB21701,30m0153mm0125m(25mL),01001g22.1:180;:300;:40(6min)10Pmin150(0min)20Pmin200(0min);:10mLPmin;MAKEUP:20mLPmin;:30mLPmin;:300mLPmin;:1L2.21.00g(0.001g),10mLDMA,20min,,2mL,2.31,2,3,4,5mL10mL,DMA1mL,2512720085ChineseJournalofAnalysisLaboratoryVol.27.Suppl.2008-52.451.00g,3mL,DMA10mL20min,,2mL,33.1,,0.99910.9993,13.2,95.4%100.9%,95.1%103.5%5%11P(gPmL)P(gPmL)P%P%124.26123.922598.6224.26123.153595.4324.26124.4032100.62.19424.26124.119699.4524.26124.4780100.92P(gPmL)P(gPmL)P%P%121.38420.338595.1221.38420.344395.1321.38420.733697.04.21421.38422.0548103.1521.38422.1237103.53.31.00g,3,2118mgPkg,2.25mgPkg()0.1%,4DMA,,,,DMA,,,,[1]GBPT5009.9822003[2]()()[3]COMMISSIONDIRECTIVE2002P72PECof6August2002relatingtoplasticmaterialsandarticlesintendedtocomein2tocontactwitffoodstuffs3512720085ChineseJournalofAnalysisLaboratoryVol.27.Suppl.2008-5