质谱仪中文操作流程（PDF52页）

Varian4000GC/MSStepByStepByFengshuangonMay.12,051…………………………………………………………2…………………………………………………………7ManualControl……………………………………………7AutoTune………………………..………………………..13………………………………………..15……………………………………..22…………………………………………………..27…………………………………………………..32……………………………………………..32……………………………………………..36……………………………………………..46………………………………………………………..4921He80psi5.5kg/cm22WorkstationToolbarsystemcontrolMSGC3Instrument1statures40003800SystemControlWorkstationToolbar344000Startup/ShutdownVacuumSystemPumpSpinSpeed35%StartUp53100%MS4Current100%300mA6BakeoutTemperatrueBakeoutTrap220Manifold120TransferLine280Holdtime812IonSource250SaveStartBakeout57DiagnosticRoughingGaugePressure50mTorr8MonitoringIonGaugeIonGaugePressure650uTorrIonGauge9DiagnosticDiagnosticTestsSelectAllStartDiagnosticPassedClearAll7ManualControl()14000TemperatureAnalysisTrap220Manifold40TransferLine280Save2TemperatureTrapManifoldTransferLineOperatingConditions583ManualControlChecksandAdjustmentsAir/WaterCheckStar4ActionMeasuringResultAcceptableLevelDone595Air/WaterCheckBakeoutAir/WaterCheck6ManualControlChecksandAdjustmentsRFRampAdjustmentStar1074000MSRF8RFBaseAmount11DONE9CalGasAdjustmentStar12104000CalibrationGas11CalibrationGasOK1-2minIon500-1000usDone13AutoTune()1AutoTuneAuto-SelectprerequisitetuningfunctionSelectAllStartAutoTuneSpectrumEventMessages220ModuleAttribude1415WorkStationView/EditMethodsOpenanexistingMethodView/EditMethod16OpenPBDE_FULLSCAN4File---Saveas175PBDE_050512PBBPBDE186MSAcquisitionMethod4000MassStarEndtimePBBPBDEGeneralParameters7IonizationControlInternalEIParametersFullScanParametersLowMass100HighMass1000198Autosampler9Injector1177InjectorOven:On,PBB&PBDETemperature250SplitRatio2010Flow/PressureConstantFlow2ml/min11ColumnOvenPBBPBDE21122214000AcquisitionActiveaMethod2OpenActiveamethod233File---NewSampleList4Save245SampleNameVialDataFile6NewFolderDataFilenamesOK257Begin8SystemControlWaiting269271Review/ProcessMSData2OpenFileReview/ProcessMSData283Search—TargetListSearchaChromatogramSelectDataFile294Open5SpectrumListAddPBB&PBDEListSelect306Done7Search318PBBPBDE321OpenFile2Quantitation—Process/ReviewRecalcList333MethodFileBrowseOpen4CalculationSetupCalibrationExternalStdReportUnkownPeaksReportMissingPeaks345CompoundTableBuildCompoundList3567361ImportCompoundListSelect2373CompoundAttributesCompoundName4Next3856CalculationsCalibrationCaliLevelAmountsResultsUnitsppm397PreviousNext8409RecalcListFileEdit4110RecalcListFile-SaveAs11Save4212DataFileBrowse13SampleTypeNewCalibBlockCalibrationCalLevel4314AutomationFileEditor15ProcessRecalcListBrowseRecalcList4416ProcessEdit17CompoundTableViewCurves4518461Review/ProcessMSData2Quantitation—ProcessActivefile473ProcessActiveFileProcess4Results485491Startup/ShutdownShutDown2TurboSpeed35StandBy502MS50340003/4()4shutdownInjectOven:Off;ColumnTemp:5051508051