离子色谱792型多点校正中文

ic_train_calib_04072002_e.ppt1•多点校正Metrohm–thewholeworldofICTrainingic_train_calib_04072002_e.ppt2Training该步骤适用于所有型号的仪器和软件系统和方法名称与校正过程无关Metrohm–thewholeworldofICic_train_calib_04072002_e.ppt3准备配置三个浓度的标准品标准11ppmF,1ppmCl,1ppmNO2标准22ppmF,2ppmCl,2ppmNO2标准35ppmF,5ppmCl,5ppmNO2Multipointcalibrationic_train_calib_04072002_e.ppt4打开ＩＣ软件Multipointcalibrationic_train_calib_04072002_e.ppt5打开系统Multipointcalibration点击:[File/Open/System]ic_train_calib_04072002_e.ppt6打开系统Multipointcalibration双击系统文件夹ic_train_calib_04072002_e.ppt7打开系统Multipointcalibration双击需要校正的系统ic_train_calib_04072002_e.ppt8打开系统Multipointcalibration屏幕上出现所选系统ic_train_calib_04072002_e.ppt9连接系统Multipointcalibration点击:[Connecttoworkplace]ic_train_calib_04072002_e.ppt10启动硬件Multipointcalibration点击:[Startuphardware(Measurebaseline)]ic_train_calib_04072002_e.ppt11启动硬件Multipointcalibration蠕动泵启动高压泵开始白色屏幕可以监测基线每20min切换一下抑制器每个位置都得到再生和冲洗大约１小时左右仪器可以开始测定ic_train_calib_04072002_e.ppt12分析标准１Multipointcalibration点击:[Startdetermination]ic_train_calib_04072002_e.ppt13Multipointcalibration填入以下信息[Ident]标识=Standard1[Calibrationlevel]校正水平=1[Info1]信息=Ｆ=1,Ｃｌ=1，ＮＯ２=1ppm[Volume]体积=定量环的体积点击：OK分析标准1ic_train_calib_04072002_e.ppt14MultipointcalibrationVerifysample分析标准1ic_train_calib_04072002_e.ppt15Multipointcalibration充满样品环–点击:[Fill]分析标准1ic_train_calib_04072002_e.ppt16Multipointcalibration抑制器自动切换用标准品１充满样品环分析标准1ic_train_calib_04072002_e.ppt17点击:[Inject]Multipointcalibration分析标准1ic_train_calib_04072002_e.ppt18Multipointcalibration窗口变蓝分析完成后自动关闭窗口标准１分析完成分析标准1ic_train_calib_04072002_e.ppt19Multipointcalibration点击:[Control/Startdetermination]类似标准１填写标准２信息点击:[OK]点击:[Fill]用标准２充满样品环点击:[Inject]分析开始直到窗口关闭，样品２分析完成分析标准2ic_train_calib_04072002_e.ppt20填写样品信息Multipointcalibration分析标准2ic_train_calib_04072002_e.ppt21Multipointcalibration点击:[Control/Startdetermination]填写标准３信息点击:[OK]点击:[Fill]充满样品环点击:[Inject]分析标准3ic_train_calib_04072002_e.ppt22填写样品信息Multipointcalibration分析标准3ic_train_calib_04072002_e.ppt23点击:[File/Open/Chromatogram]Multipointcalibration峰积分ic_train_calib_04072002_e.ppt24双击标准１:[Standard1]Multipointcalibration峰积分ic_train_calib_04072002_e.ppt25对积分结果不满意可优化积分参数Multipointcalibration峰积分ic_train_calib_04072002_e.ppt26点击“积分参数”MultipointcalibrationIntegrationofpeaksic_train_calib_04072002_e.ppt27如果自动积分结果令人满意，无需人工调整积分参数。优化参数«delay»,«width»和«slope»一般可以解决大部分的积分问题。把最小高度«minheight»调到大约0.01µS/cm;可以忽略噪音引起的峰Multipointcalibration峰积分ic_train_calib_04072002_e.ppt28积分参数调整Multipointcalibration峰积分ic_train_calib_04072002_e.ppt29必要时点击:[Events]Multipointcalibration峰积分ic_train_calib_04072002_e.ppt30点击:[Add]MultipointcalibrationIntegrationofpeaksic_train_calib_04072002_e.ppt31点击:[Enablevalley-to-valley]MultipointcalibrationIntegrationofpeaksic_train_calib_04072002_e.ppt32标准1积分参数优化后结果MultipointcalibrationIntegrationofpeaksic_train_calib_04072002_e.ppt33点击:[Components]Multipointcalibration组分ic_train_calib_04072002_e.ppt34点击三次[Add]Multipointcalibration组分ic_train_calib_04072002_e.ppt35如果所有组分都存在，确认一下是否正确标记Multipointcalibration组分ic_train_calib_04072002_e.ppt36峰标识正确敲入组分名称，比如第一个组分为氟离子可参考色谱柱说明书中的顺序来定义色谱峰。Multipointcalibration组分ic_train_calib_04072002_e.ppt37点击:[Concentrations]Multipointcalibration校正ic_train_calib_04072002_e.ppt38输入单位单位对计算结果无影响，只是显示在报告中。Multipointcalibration校正ic_train_calib_04072002_e.ppt39点击:[Add]添加校正水平Multipointcalibration校正ic_train_calib_04072002_e.ppt40点击:[OK]MultipointcalibrationCalibrationic_train_calib_04072002_e.ppt41点击:[Add]按照同样方法加入水平２和３.这样可看到３个校正水平.Multipointcalibration校正ic_train_calib_04072002_e.ppt42输入浓度.Multipointcalibration校正ic_train_calib_04072002_e.ppt43点击:[OK]关闭浓度表MultipointcalibrationCalibrationic_train_calib_04072002_e.ppt44点击:[OK]Multipointcalibration校正ic_train_calib_04072002_e.ppt45点击Appearence设置外观为[Compo-nentname+Quantity].[OK]后退出Multipointcalibration校正ic_train_calib_04072002_e.ppt46关闭窗口ICNet会询问是否保存修改Clickon:[Yes]Multipointcalibration校正ic_train_calib_04072002_e.ppt47ICNet询问是否保存方法的修改Clickon:[Yes].Multipointcalibration校正ic_train_calib_04072002_e.ppt48保存方法意味着所有新的谱图都按照所存的参数和组分记录Multipointcalibration校正ic_train_calib_04072002_e.ppt49Clickon:[Save]MultipointcalibrationCalibrationic_train_calib_04072002_e.ppt50Clickon:[Yes]MultipointcalibrationCalibrationic_train_calib_04072002_e.ppt51打开色谱图:[Openchromatogram]Multipointcalibration批处理ic_train_calib_04072002_e.ppt52选中三个色谱图.Multipointcalibration批处理ic_train_calib_04072002_e.ppt53Clickon:[ToBatch]MultipointcalibrationBatchreprocessic_train_calib_04072002_e.ppt54写不写名字都可点击ｏｋ.Multipointcalibration批处理ic_train_calib_04072002_e.ppt55点击:[Yes]覆盖原有批处理MultipointcalibrationBatchreprocessic_train_calib_04072002_e.ppt56选择标准１[Standard1].因为这个谱图的参数被修改且保存过.MultipointcalibrationBatchreprocessic_train_calib_04072002_e.ppt57Clickon:[Editsampletable]MultipointcalibrationBatchreprocessic_train_calib_04072002_e.ppt58确认样品表中的参数OK.如有不符之处可在此修改MultipointcalibrationBatchreprocessic_train_calib_04072002_e.ppt59Clickonthe«checkmarkbutton»MultipointcalibrationBatchreprocessic_train_calib_04072002_e.pp