有机反应的后处理小结

WorkupofOrg.Reaction有机反应的后处理July2011STRICTLYCONFIDENTIAL2020/11/6CONFIDENTIALCONFIDENTIAL主要内容◆后处理和评价标准◆后处理的常规方法◆常见特殊试剂的淬灭及处理◆不同溶剂反应的处理◆萃取操作◆酸碱化处理◆易燃易爆或剧毒品的后处理◆后处理常见问题的解决技巧2020/11/61CONFIDENTIALCONFIDENTIAL22020/11/6CONFIDENTIALCONFIDENTIAL2020/11/63CONFIDENTIALCONFIDENTIAL后处理的评价标准2020/11/64CONFIDENTIALCONFIDENTIAL后处理的常规方法2020/11/65CONFIDENTIALCONFIDENTIAL2020/11/66CONFIDENTIALCONFIDENTIAL2020/11/67CONFIDENTIALCONFIDENTIAL82020/11/6CONFIDENTIALCONFIDENTIAL2020/11/69CONFIDENTIALCONFIDENTIAL2020/11/610CONFIDENTIALCONFIDENTIAL2020/11/611CONFIDENTIALCONFIDENTIAL常见特殊试剂的淬灭及处理2020/11/612CONFIDENTIALCONFIDENTIAL常见特殊试剂的淬灭及处理2020/11/613CONFIDENTIALCONFIDENTIAL常见特殊试剂的淬灭及处理2020/11/614CONFIDENTIALCONFIDENTIAL常见特殊试剂的淬灭及处理2020/11/615CONFIDENTIALCONFIDENTIAL常见特殊试剂的淬灭及处理2020/11/616CONFIDENTIALCONFIDENTIAL常见特殊试剂的淬灭及处理2020/11/617CONFIDENTIALCONFIDENTIAL不同溶剂反应的处理2020/11/618CONFIDENTIALCONFIDENTIAL萃取操作2020/11/619CONFIDENTIALCONFIDENTIAL萃取操作2020/11/620CONFIDENTIALCONFIDENTIAL萃取操作2020/11/621CONFIDENTIALCONFIDENTIAL萃取操作2020/11/622CONFIDENTIALCONFIDENTIAL酸碱化处理2020/11/623CONFIDENTIALCONFIDENTIAL酸碱化处理2020/11/624CONFIDENTIALCONFIDENTIAL易燃易爆或剧毒品的后处理2020/11/625CONFIDENTIALCONFIDENTIAL易燃易爆或剧毒品的后处理2020/11/626CONFIDENTIALCONFIDENTIAL易燃易爆或剧毒品的后处理2020/11/627CONFIDENTIALCONFIDENTIAL后处理常见问题的解决技巧2020/11/628CONFIDENTIALCONFIDENTIAL后处理常见问题的解决技巧2020/11/629CONFIDENTIALCONFIDENTIALQuiz1.简单计算，淬灭剂水的用量是LAH摩尔数的多少倍，可使生成颗粒状沉淀的偏铝酸锂LiAlO2而便于过滤：a.)1;b.)2;C.)3;d.)43.下列有机溶剂中，哪种可用来除去绝大部分的BoronCompounds：a.)EtOAc;b.)MeOH;C.)EtOH;d.)CH3COCH32.萃取的次数，通常是几次：a.)1;b.)2;C.)3;d.)44.下列催化氢化催化剂中，燃烧危险性最高的是：a.)RaneyNi;b.)Pd(OH)2;C.)Pd/C2020/11/630CONFIDENTIALCONFIDENTIALTheEndThanks#answer1.)b;2.)c;3.)b;4.)a2020/11/631