DB13T 1081.16-2009 食品用包装材料及制品 塑料 第16部分己内酰胺及己内酰胺盐特定

ICS67.250X08DB13rp1DB13/T1081.16-200916Foodpackagingmaterialsandarticles-Plastics-Determinationofcaprolactamandcaprolactamsaltinfoodsimulants2009-05-272009-06-11ALDB13/T1081.16-2009liDB13/T10813112341,3567891011111213A143,3342151,31617181,21,31,4.4,4'4,4'192N,N20212223242541261272,4,61,3,5281,1,129163063123DB13/T108116DDCENS13130-1:2005ADB13/T1081.16-2009DB13/T1081.16-2009165.0mg/kg(mg/L)DB13/T1081.1-200916GB/T6682GB/T6682-2008,ISO3696:1987,MOD)o3.13%(w/v10%(v/vpH4.5pH_4.53.25GB/T66825.1:CAS105-60-2990/0.5.22:CAS935-30-898%.5.3DB13/T1081.16-20095.4555.65.75.83Y6(w/v30g0.1g5.5)IL5.910%(v/v100mL(5.6)1L5.101+2)100mL(5.6200mL5.11(500mg/L)50mg(5.1)0.1mg)(5.3)100mL,435.12350mg/L)35mg20.1mg)(5.3)100mLo435.130mL,1.0mL,2.0mL,4.0mL,6.0mL,8.0mL(5.11)25mL5.0mL(5.12)5.3)0.00mg/L,20.0mg/L,40.0mg/L,80.0mg/L,120mg/L,160mg/L270.0mg/La410.0001g,0.01go10mLo0q00b07.17.1.1120mmx120mm610mmDB13/T1081.1-20097.1.2100mL0.5cmDB131081.1-20097.27.2.1DB13/T1081.1-2009+4¡ãC7.2.24.0mL10mL1.0mL5.13),1mL7.2.38g0.1g2.0mL(5.13),mL(5.4),8mLDB13/T1081.16-2009(5.10)10min30min5mL-F7.37.3.11.0mL(5.13)610mL4.0mL0.00mg/L,5.00mg/L,10.0mg/L,20.0mg/L,30.0mg/L,40.0mg17.5mg/L3%(w/v(5.810%(v/v(5.9)7.3.28g0.1g62.0mL(5.13),0.00mg/kg,5.00mg/kg,10.0mg/kg,20.0mg/kg,30.0mg/kg,40.0mg/kg,17.5mg/kg15mL(5.4),8mL(5.10)10min30min5mL7.47.2881a)30mX0.32mm1¦Ìmb)80,C30C/min230¡ãCmin;c)230*C;d)280*C;e)fl1mL/min;g)0.5minh)1.0¦ÌL08.28.1(7.3)2A01)y=(axx)+b(1)2mg/Lmg/kg);b0.996099.1C2)DB13/T1081.16-2009bU(2)aCPAmg/Lmg/kg);2b-9.29.2.13)M=CxV(3)Ax1000Mmg/dm2;Cmg/L;VmL;Adm209.2.24)M=C............................................................(4)Mmg/L;Cmg/L09.2.3mg/kgmg/dmDB13/T1081.1-2009131010%011GC-MS)2.0mL2.0mLGC-MSGC-MSSIM)m30,55,84113100:70:50:45DB13/T1081.16-2009A(mi12.2A.1(15.0mg/kg