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ICS67.250X08DB13AjtDB13/T1081.5-20095Foodpackagingmaterialsandarticles-Plastics-Determinationofvinylidenechlorideinfoodsimulants2009-05-272009-06-11dDB13/T1081.5-2009IjDB13/T10813112341,3567891011111213A143,3342-Ail151,31617181,2.1,31,44,454,4'192N,N20212223242541261272,4,61,3,5281,1,129163063123DB13/T10815DDCEN/TS13130-1:2005ABDB13/T1081.5-2009DB13/T1081.5-20095001mg/L,0.001mg/kg2DB13/T1081.1-20091GB/T6682GB/T6682-2008,ISO3696:1987,MOD)33.13%(w/v%(v/vpH4.5pH4.53.245GB/T66825.15000mg/L5.2N,N99%05.35.4DB13/T1081.5-20095.55.63%(w/v.0g0.1g(5.3500mL5.710%(v/v50mL(5.4)500mL5.8710mL(6.210mLN,N(5.2)0¦ÌL.5L.10¦ÌL.20L.30¦ÌL,40L.50L5.1),5.2N,N0mg/L.2.5mg/L.5mg/L.10mg.15mg/L.20mg25mg5.999.999%.66.16.26.36.46.510mL20mL10L.25.50¦ÌL,0.0001g,0.01go77.17.1.1120mmx120mm610mmDB13/T1081.1-20097.1.2100mL0.5cmDB13/T1081.1-20097.27.2.1lOmL20mL6.3)7.2.2lOg¡Àlg(5.5)20mL(6.3)7.37.3.16(6.3)lOmL2.5mg/L,5mg/L,10mg/L.15mg/L,20mg/L,25mg/L5.8)20L0.005mg/L,0.01mg/L.0.02mg/L.0.03mg/L,0.04mg/L0.05mg/L3%(wN109/0(v/vDB13/T1081.5-20097.3.210g0.1g66.3)2.5mg/L,5mg/L,10mg/L,15mg/L,20mg/L,25mg/L5.8)20L0.005mg/L,0.01mg/L,0.02mg,0.03mg/L,0.04mg/L0.05mg/L47.47.38.1a)30mX0.32mm,1¦Ìmob)407C1min2¡ãC/min60CImin,20200¡ãC1min.c)200¡ãC1mind)200¡ãCoe)(5.9)¡ãf)1.0mL/minog)1B.8.27.3(7.3)A.1)y=(axx)+b(1)l-mg/Lmg/kg);ab0.996.C2)!'+Y-b(2)aCmg/Lmg/kg);JDB13/T1081.5-2009b-9.29.2.13)M=CxV(3)Ax1000Mmg/dm2;Cmg/L;VmL;Adm2o9.2.24)M=C............................................................(4)Mmg/L;Cmg/L.9.2.3mg/kgmg/dm2DB13/T1081.1-2009131010%,11GC-MS)GC-MSm/z9698DB13/T1081.5-2009A11eseswees1A.1jat]10.CJolJC3.C1.01mg/LDB13/T1081.5-2009B70¡ãC1¡ãC30minBB351mL