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ICP-MS198027ICP-MSICP-MS(10-1510-12)89AsSeHgCVGCVG-ICP-MSICP-MSICP-MSSnCl2KBH4VisPhoto-HCOOHUVphoto-HCOOHICP-MSICP-MSKBH42.5105L-1KBH4SnCl2VisPhoto-HCOOHUVphoto-HCOOH0.0020.0010.003gL-1KBH40.01gL-1KBH4H2ICP-MSKBH4KBH40.05gL-1SnCl2HCOOHKBH4HCOOHHCOOHHCOOHUV-CVGHCOOHKBH4SnCl2HCOOHFe3+Co2+Ni2+Cu2+Zn2+Pb2+1000KBH4SnCl2HCOOH298-107HCOOHUVphoto-CVG-ICP-MSICP-MSICP-MSICP-MSAsCdHgPbAsHClO4HClO4AsAsCdHgPb1-494-10583-114CaNaMgCuAlFeICP-OESICP-OESAsHG-AFSAsICP-MSICP-OESICP-MSICP-MSICP-MS27AsCdHgPb-,,-,(1),-,-(2),,8min0.10-20.00ng/mL,0.025g/kg(3)6(),ESIMRM,20min10.00-200.00ng/mL,,2.0g/kg,(4)HPLC-MS/MS,ESIMRM,15min0.0110.00mg/L,,0.05mg/kg,0.1mg/kg,-(UPLC-TOF-MS),,,1.UPLC-TOF-MSMasslynx,,1196(),Masslynx,2.21010mLOasisHLBDirectConnectHPUPLC-Q-TOF,,194(92%)(LOD)100ng/L,,(70%)80%,(RSD%,n=6)30%3.133,QuEChERSQuEChERS12580%,,/()2009,..,,,,GC/MS-EIGC/MS-NCI.,.,HPLC/MS/MS.,.,,GC/ECDGC/MS,.()(),,.,()-,1082,,-,(HPLC)1-4,,,,,HPLC-1-415min,AgilentZorbaxXB-C18,0.1%(1585,VV)ESI,,4lng/mL,5100ng/mL,85%-97%(GPC)-HPLC-(MS/MS)1-4GBG7B,10GPCHPLC,InertsilC18,,3,(LOD)0.1-1.8ng/g,(LOQ)0.45.0ng/g.10581.7-92.9%(RSDs)2.9-7.8%3.9-8.1%,(SPE)-HPLC-MS/MS8,SCX,HPLC-MS/MS,2002657EC80.10.5lg/kg87.3-117%,3.35-10.1%,3.21-10.3%8(decisionlimit,CCa)0.029-0.049g/kg,(detectioncapability,CC0.0490.083g/kgoSPE-HPLC-MS/MS-(8020,vv),OasisMAX,,,(r2)0.98993-473.0%-95.7%,3.29%-9.87%,(LOD)0.008g/kg,(LOQ)0.02g/kgGPC-HPLC-MS/MS2,,,,11000g/kg,,0.992184.6%-103%,2.64%-8.82%,LOD10g/kg,3g/kgLOQ20g/kg,10g/kg,-1.2.GPCSPE3.4.,,,,5.,,,,6.CCCCIUPAC2002657EC