萃取精馏及进展

1999-11-011971-!!!!!!!!!!!!!!!!300072TG028.3+2A1004-9533200104-0215-06TG028.1+3ExtractivedistillationanditsdevelopmentCUIXian-baoYANGZhi-caiFENGTian-yangSchoolofChemicalEngineeringTianjinUniversityTianjin300072ChinaAbstractExtractivedistillationisawell-knowntechnigueforseparatingazeotropesandmix-turesofcomponetshavingcloseboilingpoint.Extractivedistillationincludescontinuousdistil-lationandbatchextractivedistillation.Thebatchextractivedistillationisanewtechniguede-velopedrecently.Theselectionofsolventforextractivedistillationisthekeyaspectfortheex-tractivedistillationprocess.Inthepasttimethesolventusedforextractivedistillationissinglesolvent.~oweverinrecentyearsthemixedsolventisstudiedandusedbecauseofitsgoodfea-tures.Keywordsextractivedistillationbatchextractivedistillationmixedsolvent20018Aug.2001C~EMICALINDUSTRYANDENGINEERING184Vol.18No.41!!!12!456726-82910-1131241314!#15!171!51!==02!=!03A!!04BS!=0LANGP17a234b223abc3361220018LANGP1SAFRIT181932SAFRIT-12!d#e$b!!CEDBED123456!#712184!=!!!#!!!##MOMOHSO202.2BROWNLEE2123-23-DMPCyC61CyC623-DMP1l23-CyC623-DMP-0.842001.02671.06571.07N-571.07181.22BROWN22CyC522-22-DMBN---2-NMEPCHOLN--NMP222-22-50ANMEPCHOL911BNMEPCHOL411CNMEPNMP911222-!CyC522-DMB311NMEP1.28311ANMEP+CHOL1.40311BNMEP+CHOL1.42311CNMEP+NMP1.32511NMEP1.48511CHOL1.32511NMP1.37511ANMEP+CHOL1.64511BNMEP+CHOL1.57511CNMEP+NMP1.54711NMEP1.71711CHOL1.26711NMP1.33711ANMEP+CHOL1.70711BNMEP+CHOL1.64711CNMEP+NMP1.7428122001823C8C837.5%4.7%11.7%7.1%19%5.9%14.1%1.03!01.01.31.3101.62.22.2101.82.52.5LeeFM7.5mm720mm45cm3!min420mm630mm450cm3!min99.9%4LEEFM2426!%0.260.40!1X10-40.220.23!1X10-435.8136.54!1X10-43.733.95!1X10-412.0313.47!1X10-42.973.13!1X10-47.457.84!1X10-44.525.79!1X10-40.03950.0431!1X10-423.8218.911.680.03900.057315X10-48.939.57!1X10-400.3798.301BENEDICTM.RUBINRL.Extractiveandazeo-tropicdistillationJ.TransamInstChemEng194541353-370.9121842DUNNCLMILLARRWPEIROTTIGetal.ToluenerecoverybyextractivedistillationJ.TransAmInstChemEng194541631-644.3HENNIGRWEISSS.Zumaustauschgradbeiderextraktivdestillationambeisielderbenzengewin-nungauseinerbenzinfrakionJ.ChemTechLeipzig1988405195-198.4.J.199523249-61.5BERGL.Sparationof!-xylenefrom-xyleneor#-xylenebyextractivedistillationwithalcoholsP.US50947231992-05-10.6BERGL.Sparationofxylenesbyextractivedistil-lationP.US54416081995-08-15.7RITTNERSSCHMIDTASTEINERRetal.Ver-fahrenzurtrennungvon!-und-DichlorobenzolP.EP4517201991-05-04.8VILASGGAUTAMKS.Extractivedistillationof-Cresols!26-xylenolmixturesinthepresenceofalkanolaminesJ.SepSciTechnol199631141979-1988.9BERGLVOSBURGHMG.SeparationofethanolfromisopropanolbyextractivedistillationP.US47102741987-12-01.10CEPEDAERESAJM.SeparationbyextractivedistillationofmixturesofalcoholsandtheestersofaceticacidISolventSelectionJ.IntChemEng1994344481-485.11.J.199310446-50.12BERGLWYTCHERLEYRW.Separationoffor-micacidfromaceticacidbyextractivedistillationP.US52270291993-07-13.13.C5J.19972825-9.14RUIZCCOCAJVEGAAetal.Extractivedistil-lationofhydrocarbonswithdimethylformamideex-perimentalandSimulationdataJ.IndEngChemRes1997364934-4939.15LANGPYATIMPOSZKOWICZPetal.BatchextractivedistillationunderconstantrefluxRatioJ.computersChemEngng19941811!121057-1069.16LELKESZLANGPMOSZKOWICZPetal.BatchextractivedistillationtheprocessandtheoperationalpoliciesJ.ChemEngSci19985371331-1348.17LANGPLELKESZMOSZKOWICZPetal.Dif-ferentoperationalpoliciesforthebatchextractivedistillationJ.ComputersChemEngng199519S645-650.18SAFRITBTWESTERBERGAW.ExtendingcontiuousconventionalandextractivedistillationfeasibilityinsightstobatchdistillationJ.IndEngChemRes1995343257-3264.19SAFRITBTWESTERBERGAW.Improvedop-erationalpoliciesforbatchextractivedistillationJ.IndEngChemRes199734436-443.20MOMOHSO.Assessingtheaccuracyofselectivityasabasisforsolventscreeninginextractivedistil-lationProcessJ.SepSciTech1991265729-742.21LEEFMBROWNRE.ExtractivedistillationofhydrocarbonsemployingsolventmixtureP.US49215811990-05-01.22BROWNRELEEFM.ExtractivedistillationofhydrocabonfeedsemployingmixedsolventP.US49542241990-09-04.23LEEFMGENTRYJC.DontoverlookextractivedistillationJ.ChemEngProg1997931056-64.24LEEFMBROWNRE.ExtractivedistillationofhydrocarbonmixturesemployingmixedsolventP.US49484721990-08-14.25LEEFM.Extractivedistillationofcycloalkane!al-kanefeedemployingmixedsolventP.US49448491990-07-31.26LEEFM.ExtractiveDistillationofalkane!cycloal-kanefeedemployingmixedsolventP.US49484701990-08-14.02220018萃取精馏及进展作者：崔现宝，杨志才，冯天扬作者单位：天津大学化工学院,刊名：化学工业与工程英文刊名：CHEMICALINDUSTRYANDENGINEERING年，卷(期)：2001,18(4)被引用次数：25次参考文献(26条)1.BENEDICTM;RUBINRLExtractiveandazeotropicdistillation19452.DUNNCL;MILLARRW;PEIROTTIGToluenerecoverybyextractivedistillation19453.HENNIGR;WEISSSZumaustauschgradbeiderextraktivdestillationambeisielderbenzengewinnungauseinerbenzinfrakion1988(05)4.郑英峨;姜华;赵维彭萃取精馏法分离焦化苯中微量正庚烷精馏塔计算1995(02)5.BergLSparationofm-xylenefromp-xyleneoro-xylenebyextractivedistillationwithalcohols19926.BergLSparationofxylenesbyextractivedistillation19957.RITTNERS;SCHMIDTA;SteinerRVerfahrenzurtrennungvonm-undp-Dichlorobenzol19918.VilasG;GAUT