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ICS73.060.20D32GB/T24519-2009XManganeseores-Determinationofmagnesium,aluminum,silicon,phosphorus,sulfur,potassium,calcium,titanium,manganese,iron,nickel,copper,zinc,bariumandleadcontent-WavelengthdispersiveX-rayfluorescencespectrometricmethod2009-10-302010-05-01R-R512C.GB/T24519-2009ABCGB/T24519-2009xX1,1AA120,0.24-9.78BaO0.08-2.96CaO0.09-19.8CuO0.012-0.045Fee031.8-30.0K200.02---4.99MgO0.04-3.82MnO20.33-75.9NiO0.03-0.13P20S0.066-0.619PbO0.003-0.25Si022.0-47.6SO30.018-0.67TiO20.04-0.54ZnO0.005---0.1992GB/T2011GB/T6379.11GB/T6379.1-2004,ISO5725-1:1994,IDT)GB/T6379.22GB/T24519-2009GB/T6379.2-2004,ISO5725-2:1994,IDT)GB/T6682GB/T6682-2008,ISO3696:1987,MOD)GB/T14949.8GB/T14949.8-1994,eqvISO310:1981)GB/T16597X3XX4GB/T66824.1Li,B,0LiBO67:3365:35,50:50,12:22,35:656504h4.2LiNO3NH4NO3,NaNO34.3NH,ILiI,LiBrLiBr1052h.4.4LiNO3220mg/mL,LiBr10mg/mLNH,I60mg/mL220gLiNO3,10gLiBr60gNH4I500mL1000mL,51jJS5.45.5XGB/T1659795%R+5%Au)30mL,95YoR+50oAu)1100C,0.1mg,6GB/T2011100¦Ìm7A7.1AAGB/T14949.87.2f5.2),10505.4).6000g6,6.0000g(4.1)0.2mg1mL(4.4)1050(5.4)10min(5.2GB/T24519-2009(Lf1mL4.4),Lf1)LM2X100¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤1)MIg);m2g);mfg).L2)L=!4X10RXLf..............................(2)m3g);m4g);myg);R10;Lf8A0.6000a)6(5.2)0.2mg100JL6.0000g4.1),1mL4.4),b)0.600066.0000g(4.1)0.2mg,1mL(4.4),La)b)8.2105010min3min1231050r-.3GB/T24519-200999.130a8.la)9.2it34A9.3aa3B1BrLaBrLaAl10f10.110.2Itx3)CCm;x(100-L)/(100-A)..............................(3)ClCm;%;LA(4C;=CmX100/(100-A).........................¡¤4)ClC.4GB/T24519-2009A-11C,1288GB/T6379.1GB/T6379.22,A21Ht¡ãarRAlp030.0048m0.0421R=0.0088m+0.0621BaOr=0.0238m-0.0003R=0.0547m-0.0014CaOr=0.0044m+0.0055R=O.0116+0.0257CuOr0.0432m0.0016R=0.0962m0.0046Fee030.0058m+0.0116R=O.0098m+0.0474KZOr=0.0224m-0.0009R=0.0416m+0.0075MgOr=0.0215m0.0038R=O.0357m+0.0167MnOr=0.1970R=O.3310NiOr=0.039lm+0.0014R=0.0592m+0.0023PZO;=0.119Om+0.0008R=O.117lm+0.0084PbOr=0.0067m+0.0036R=O.039Om+O.0042SiO2r=0.003Om+O.0687R=0.0059m+0.1064SO3=0.0227m+0.0059R=0.0614m+0.0087TiOZ=0.0062m0.0047R=0.0037m+0.0080ZnOr=0.0052m+0.0021R=0.01200.0034m13a)bc)d)e)f)ghi)GB/T24519-2009AmfA.1ItA.1A.1f12kVmAsAle03AlKaPET0.46145.000139.3233010630EaOBaKaLiF2000.1587.17889.498506420CaOCaKaLiF2000.46113.165115.067506420CuOCuKaLiF2000.1545.01844.330605320FezO,FeKaLiF2000.1557.522604020K2OKKaLiF2000.46136.746138.716506420MgOMgKaOVO-550.4620.86419.57122.1953010630MnOMnKaLiF2000.1562.982502030NiONiKaLiF2000.1548.66048.02649.579605320P,O,PKGe0.46140.972142.6713010630PbOPbLLiF2000.1528.23527.62128.991605320SiO2SiKaInSb0.46144.602147.0603010620SO3SKaGe0.46110.631113.5573010630TiO2TiKaLiF2000.4686.19283.883506020ZnOZnKaLiF2000.1541.78541.08342.665605320A.2A.1)In=IP¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤A.1)IIPI6A.2)In=I(IB,XBIXB,)/(BB,¡¤........(A.2)I.XIPXIRI11B21,2X6GB/T24519-2009B1,B21,22020A.3AA.3)C'2300X(4xt,+IbXtb)''Z)/(IPXtp+IbXtb...............(A.3)CVI,Ibtptbtt,x(Ih/IP)t/2A.2,A.20.01%n0.011¡ã%110%10%-20¡ãa20%10310.30.1GB/T24519-2009sRBB.1),C,=sX(1+zaqXC1)X(I;+XIk)+bC;,C3s,ba33aI;X(B.1)GB/T24519-2009CC.1C.1ItfAlp03Al0.5293BaOBa0.8957CaOCa0.7147CuOCu0.7989Fe203Fe0.6994KZOK0.8301MgOMg0.6030MnOMn0.7745NiONi0.7858Pz0sP0.4364PbOPb0.9283SiO2Si0.4674SO3S0.4005TiO2Ti0.5993ZnOZn0.8035600160AItXGB/T24519-200916:100045¡¤1-3938618.00GB/T24519-2009(010)68533533